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This collection of reports demonstrate the extensive purview of NMR and its applications. The pellucid presentations provided include accounts on application of NMR spectroscopy to sciences and technologies of glassand ceramics; high-resolution solid-state NMR studies on ceramics; NMR studies of zeolite; NMR studies of higher-order structures of solid polymers; and organic thin films. Taken together with reviews in other volumes of this series, the present accountsably demonstrate that NMR is facile princeps when it comes to problem solving in most areas of science, including the medical sciences. Read more... Abstract: This collection of reports demonstrate the extensive purview of NMR and its applications. The pellucid presentations provided include accounts on application of NMR spectroscopy to sciences and technologies of glassand ceramics; high-resolution solid-state NMR studies on ceramics; NMR studies of zeolite; NMR studies of higher-order structures of solid polymers; and organic thin films. Taken together with reviews in other volumes of this series, the present accountsably demonstrate that NMR is facile princeps when it comes to problem solving in most areas of science, including the medical sciences
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ANNUAL REPORTS ON
NMR SPECTROSCOPY Edited by I. ANDO" and G. A. WEBBY *Department of Polymer Chemistry, Tokyo Institute of Technology, Ookayama, Meguro-ku, Tokyo, Japan WDepartment of Chemistry, University of Surrey, Guildford, Surrey, England
VOLUME 28
ACADEMIC PRESS Harcoutt Brace & Company, Publishers London 0 San Diego New York Boston 0 Sydney 0 Tokyo Toronto
ACADEMIC PRESS LIMITED 24-28 Oval Road, LONDON NW17DX
U.S. Edition Published by ACADEMIC PRESS INC. San Diego, CA 92101 This book is printed on acid free paper
Copyright 0 1994 ACADEMIC PRESS LIMITED
AN Rights Reserved
N o part of this book may be reproduced or transmitted in any form or by any means, electronic or mechanical including photocopying, recording, or any information storage and retrieval system without permission in writing from the publisher A catalogue record for this book is available from the British Library
ISBN 0-12-505328-2 ISSN 0066-4103
Phototypesetting by Keyset Composition, Colchester, Essex Printed by Hartnolls Limited, Bodmin, Cornwall
LIST OF CONTRIBUTORS I . Ando, Department of Polymer Chemistry, Tokyo Institute of Technology, Ookayama, Meguro-ku, Tokyo, Japan. S . Ando, NTT Interdisciplinary Research Laboratories, Midori-cho, Musashino-shi, Tokyo, Japan.
F. D . Blum, Department of Chemistry and Materials Research Center, University of Missouri-Rolla, Rolla, MO 65401, USA. H . Ernst, Universitat Leipzig, Fachbreich Physik, Linnkstr. 5 , 04103 Leiprig, Germany. S . Hayashi, National Chemical Laboratory for Industry, Tsukuba, Ibaraki 305,Japan.
H . Kawazoe, Research Laboratory of Engineering Materials, Tokyo Institute of Technology, Natatsuta, Midori-ku, Yokohama 227, Japan.
H . Kurosu, Department of Polymer Chemistry, Tokyo Institute of Technology, Ookayama, Meguro-ku, Tokyo, Japan. H . Pfeifer, Universitat Leipzig, Fachbreich Physik, Linnkstr. 5 , 04103 Leipzig, Germany. H . Yoshimizu, Department of Materials Science and Engineering, Nagoya Institute of Technology, Gokiso-cho, Showa-ku, Nagoya, Japan.
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PREFACE This is the first of a series of special issues of Annual Reports on NMR Spectroscopy, and it is devoted to Applications of NMR to New Materials. It is a great pleasure for me to welcome as co-editor of this issue Professor I. Ando of the Tokyo Institute of Technology. Professor Ando and I have cooperated in many areas of NMR over the past 15 years and I am especially happy to have been able to draw upon his considerable knowledge of new mat