E-Book Overview
Micro process engineering is approaching both academia and industry. With the provision of micro devices and systems by commercial suppliers, one main barrier for using these units has been eliminated. More and more they become familiar, thereby being one facet of the upheaval in chemical industry.This book focuses on processes rather than on devices: what is 'before' and 'behind' micro device fabrication. A comprehensive and detailed overview is given on:A multi-faceted, hierarchic analysis of chemical micro process technologyModelling and simulation of micro reactorsLiquid- and liquid/liquid-phase reactionsGas/liquid reactionsGas-phase reactions (heterogeneous catalysis)
E-Book Content
I
V. Hessel, S. Hardt, H. Löwe Chemical Micro Process Engineering
Chemical Micro Process Engineering: Fundamentals, Modelling and Reactions Volker Hessel, Steffen Hardt, Holger Löwe Copyright © 2004 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim ISBN: 3-527-30741-9
II
Related Titles V. Hessel, S. Hardt, H. Löwe
T. Gh. Dobre, J. G. Sanchez Marcano
Chemical Micro Process Engineering
Chemical Engineering
Processing, Applications and Plants 2004
Modelling, Simulation and Similitude 2004
ISBN 3-527-30607-2
ISBN 3-527-30998-5
K. Sundmacher, A. Kienle (Eds.) W. Ehrfeld, V. Hessel, H. Löwe
Reactive Distillation
Microreactors
Status and Future Directions
New Technology for Modern Chemistry 2000
2003
ISBN 3-527-30579-3
ISBN 3-527-29590-0
S. P. Nunes, K.-V. Peinemann (Eds.) W. Menz, J. Mohr, O. Paul
Membrane Technology
Microsystem Technology
in the Chemical Industry
2001
2001
ISBN 3-527-29634-4
ISBN 3-527-28485-0
J. G. Sanchez Marcano, Th. T. Tsotsis
Catalytic Membranes and Membrane Reactors 2002
ISBN 3-527-30277-8
III
Volker Hessel, Steffen Hardt, Holger Löwe
Chemical Micro Process Engineering Fundamentals, Modelling and Reactions
IV
Dr. Volker Hessel Dr. Steffen Hardt Dr. Holger Löwe IMM – Institut für Mikrotechnik Mainz GmbH Carl-Zeiss-Straße 18–20 55129 Mainz Germany
This book was carefully produced. Nevertheless, authors and publisher do not warrant the information contained therein to be free of errors. Readers are advised to keep in mind that statements, data, illustrations, procedural details or other items may inadvertently be inaccurate.
Cover Illustration
Library of Congress Card No.: Applied for. A catalogue record for this book is available from the British Library.
Upper left: Production- and pilot-scale gas/ gas counter-flow heat exchanger comprising microstructured channel arrays. The device (including flanges about 36 kg heavy and 54 cm long), made of stainless steel, is designed for gas throughput in the range of m3/min at 100 mbar pressure drop for a power of about 10 kW. The internals consist of a stack of microstructured plates having multi-channel arrays of a channel width of 2 mm, depth of 250 µm, and length of 240 mm. Totaling, 6685 micro channels are operated in parallel in this device. The flange-type connection allows installation in large-scale industrial plants (IMM MainzHechtsheim, Germany). Center: CFD simulation of streamlines of a liquid flow in a caterpillar micro mixer. This device utilizes the split-recombine principle leading to distributive mixing. It is seen that by multiple repetition of this principle the entanglement of the streams increases (IMM Mainz-Hechtsheim, Germany). Lower right: Cross-flow catalyst screening device with multiple short mini-fixed beds. The fixed-bed catalyst section is fed by bifurcation-channel flow architectures that serve for flow equipartition. This