Experimental Organic Chemistry: A Miniscale And Microscale Approach

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E-Book Overview

Providing even more emphasis on inquiry-based learning, a new green experiment, and more than a dozen new discovery experiments, this Fifth Edition of Gilbert and Martin's proven EXPERIMENTAL ORGANIC CHEMISTRY contains procedures for both miniscale (also known as small scale) and microscale users. The manual first provides an early focus on equipment, record keeping, and safety in the laboratory, then walks students step by step through the laboratory techniques they need to perform the book's experiments with confidence. Chapters show students how to use the book's techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. A bioorganic experiment in Chapter 24 reflects the increasing emphasis on bioorganic chemistry in the course and gives students an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide.

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E-Book Information

• Series: Brooks Cole Laboratory Series for Organic Chemistry

• Year: 2,010

• Edition: 5

• Pages: 966

• Pages In File: 966

• Language: English

• Topic: 300

• Issue: 2011 12 30

• Identifier: 1439049149,9781439049143

• Paginated: 1

• Org File Size: 55,301,756

• Extension: pdf

• Tags: Химия и химическая промышленность Органическая химия Синтетические и экспериментальные методы ОХ

• Toc: Front Cover......Page 1Title Page......Page 7Copyright......Page 8Table of Contents......Page 101.1 Introduction......Page 291.2 Preparing For The Laboratory......Page 301.3 Working In The Laboratory......Page 311.5 General Protocol For The Laboratory Notebook......Page 321.6 Types Of Organic Experiments And Notebook Formats......Page 331.7 Sample Calculations For Notebook Records......Page 421.8 Safe Laboratory Practice: Overview......Page 441.9 Safety: General Discussion......Page 451.10 Safety: Material Safety Data Sheets......Page 471.11 Safety: Disposal Of Chemicals......Page 49Historical Highlight: The Importance of Record Keeping......Page 522.1 Glassware: Precautions And Cleaning......Page 552.2 Standard-Taper Glassware For Miniscale Procedures......Page 562.3 Standard-Taper Glassware For Microscale Procedures......Page 572.4 Assembling Apparatus......Page 592.5 Measuring And Transferring Liquids......Page 602.6 Weighing Methods......Page 652.7 Melting-Point Methods And Apparatus......Page 662.8 Boiling-Point Methods And Apparatus......Page 692.9 Heating Methods......Page 712.10 Cooling Techniques......Page 792.11 Stirring Methods......Page 802.12 Centrifugation......Page 822.13 Simple Distillation......Page 832.14 Fractional Distillation......Page 862.15 Vacuum Distillation......Page 882.16 Steam Distillation......Page 92