E-Book Overview
Crystal Structure Analysis, Third Edition, explains how and why the detailed three-dimensional architecture of molecules can be determined by an analysis of the diffraction patterns obtained when X-rays or neutrons are scattered by the atoms in single crystals. Part 1 covers the nature of the crystalline state, diffraction in general, and diffraction by crystals, and also looks briefly at experimental procedures. Part II examines the problem of converting the experimentally obtained data into a model of the atomic arrangement that scattered these beams. Part III discusses techniques for refining the approximate structure to the degree warranted by the experimental data. It also describes the many types of information that can be obtained by modern crystal structure analysis. The text is enhanced by numerous illustrations, a detailed glossary, and several appendices that cover mathematical details.
E-Book Content
INTERNATIONAL UNION OF CRYSTALLOGRAPHY BOOK SERIES IUCr BOOK SERIES COMMITTEE
J. Bernstein, Israel G. R. Desiraju, India J. R. Helliwell, UK T. Mak, China P. Müller, USA P. Paufler, Germany H. Schenk, The Netherlands P. Spadon, Italy D. Viterbo (Chairman), Italy IUCr Monographs on Crystallography
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Accurate molecular structures A. Domenicano, I. Hargittai, editors P.P. Ewald and his dynamical theory of X-ray diffraction D.W.J. Cruickshank, H.J. Juretschke, N. Kato, editors Electron diffraction techniques, Vol. 1 J.M. Cowley, editor Electron diffraction techniques, Vol. 2 J.M. Cowley, editor The Rietveld method R.A. Young, editor Introduction to crystallographic statistics U. Shmueli, G.H. Weiss Crystallographic instrumentation L.A. Aslanov, G.V. Fetisov, J.A.K. Howard Direct phasing in crystallography C. Giacovazzo The weak hydrogen bond G.R. Desiraju, T. Steiner Defect and microstructure analysis by diffraction R.L. Snyder, J. Fiala and H.J. Bunge Dynamical theory of X-ray diffraction A. Authier The chemical bond in inorganic chemistry I.D. Brown Structure determination from powder diffraction data W.I.F. David, K. Shankland, L.B. McCusker, Ch. Baerlocher, editors
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Polymorphism in molecular crystals J. Bernstein Crystallography of modular materials G. Ferraris, E. Makovicky, S. Merlino Diffuse x-ray scattering and models of disorder T.R. Welberry Crystallography of the polymethylene chain: an inquiry into the structure of waxes D.L. Dorset Crystalline molecular complexes and compounds: structure and principles F. H. Herbstein Molecular aggregation: structure analysis and molecular simulation of crystals and liquids A. Gavezzotti Aperiodic crystals: from modulated phases to quasicrystals T. Janssen, G. Chapuis, M. de Boissieu Incommensurate crystallography S. van Smaalen Structural crystallography of inorganic oxysalts S.V. Krivovichev The nature of the hydrogen bond: outline of a comprehensive hydrogen bond theory G. Gilli, P. Gilli Macromolecular crystallization and crystal perfection N.E. Chayen, J.R. Helliwell, E.H. Snell
IUCr Texts on Crystallography
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The solid state A. Guinier, R. Julien X-ray charge densities and chemical bonding P. Coppens Fundamentals of crystallography, second edition C. Giacovazzo, editor Crystal structure refinement: a crystallographer’s guide to SHELXL P. Müller, editor Theories and techniques of crystal structure determination U. Shmueli Advanced structural inorganic chemistry Wai-Kee Li, Gong-Du Zhou, Thomas Mak Diffuse scattering and defect structure simulations: a cook book using the program DISCUS R. B. Neder, T. Proffen The basics of crystallography and diffraction, third edition C. Hammond Crystal structure analysis: principles and practice, second edition W. Clegg, editor Crystal structure analysis: a primer, third edition J.P. Glusk