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JOURNAL OF CHROMATOGRAPHY LIBRARY - volume 26 chromatography of antibiotics second, completely revised edition This Page Intentionally Left Blank JOURNAL OF CHROMATOGRAPHY LIBRARY - volume 26 chromatography of antibiotics second, completely revised edition Gerald H. Wagman Director, Microbiological Strain Laboratory, Schering Corporation, Kenilworth, New Jersey 07033, U.S.A. Matvin J. Weinstein Vice President (retired), Microbiological Research, Schering Corporation, Bloom field, New Jersey 07003, U.S.A. E LSEV I E R Amsterdam - Oxford - New York - Tokyo 1984 ELSEVIER SCIENCE PUBLISHERS B.V. Molenwerf 1 P.O. Box 21 1, 1000 AE Amsterdam, The Netherlands Distributors for the United States and Canada: ELSEVIER SCIENCE PUBLISHING COMPANY INC. 52, Vanderbilt Avenue New York, N Y 10017 Library of Congress Cataloging in Publleation Data Wagman, Gerald H. Chromatography of a n t i b i o t i c s . ( J o u r n a l of chromatography l i b r a r y ; v. 120) Includes index. 1. Antibiotics-Analysis. 2. Chromatographic analysis. I . Weinstein, Marvin J . 11. T i t l e . 111. S e r i e s . RS190.A5W33 lgc4 615'. 329 84-1464 ISBN 0-444-h;007-X ISBN 044442007-X (Val. 26) ISBN 044441616-1 (Series) 0 Elsevier Science Publishers B.V., 1984 A l l rights reserved. N o part of this publication may be reproduced, stored in a retrieval system or transmitted in any form or by any means, electronic, mechanical, photocopying, recording or otherwise, without the prior written permission of the publisher, Elsevier Science Publishers B.V., P.O. BOX 330, 1000 A 9 Amsterdam, The Netherlama. Printed in The Netherlands V Contents Journal of Chromatography Library . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Preface to the revised edition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Preface to the first edition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Acknowledgements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Abbreviations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Chromatography of antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Chromatographic classification of antibiotics . . . . . . . . . . . . . . . . . . . . . . Detection of antibiotics on chromatograms . . . . . . . . . . . . . . . . . . . . . . . Chromatographic data section . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Comments on the use of the data section . . . . . . . . . . . . . . . . . . . . . . . . . Named antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Numbered antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Compound indexes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Named antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Numbered antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . VII IX XI xi11 xv 1 3 11 19 21 23 406 471 473 50 1 This Page Intentionally Left Blank VII JOURNAL OF CHROMATOGRAPHY LIBRARY A Series of Books Devoted t o Chromatographic and Electrophoretic Techniques and their Applications Although complementary t o t h e Journal of Chromatography, each volume in the library series is an important and independent contribution in the field of chromatography and electrophoresis. The library contains no material reprirlted from the journal itself. Volume 1 Chromatography of Antibiotics (see also Volume 2 6 ) by G.H. Wagman and M.J. Weinstein Volume 2 Extraction Chro